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1 H NMR (CD 3 OD, 400 MHz) δ 10.03 (s, 1H), 8.41 (d, J = 9.6 Hz, 1H), 8.25 (d, J = 9.6 Hz, 1H), 7.81 (d, J = 9.6 Hz, 1H), 7.68 (dd, J = 9.2, 2.8 Hz, 1H), 7.61 (d, J = 1.6 Hz, 1H), 7.52 (d, J = 2.8 Hz, 1H), 7.42–7.37 (m, 2H), 4.85–4.81 (m, 1H), 3.81–3.75 (m, 2H), 3.65–3.59 (m, 1H), 3.45–3.38 (m, 2H), 3.28–3.21 (m, 4H), 2.77–2.72 (m, 1H)